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Oxygen and moisture measurement in 3D printing

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Panametrics' Customer Story
oxy.IQ Fuel Cell Oxygen Analyzers

3D printing is expected to show significant growth in the coming years. The process of 3D printing involves applying layers of fine dust metals or polymers and then fusing the layers with laser technology. The process takes place in the chamber of the 3D printing machine where the environment is closely monitored for oxygen and moisture content. Excess moisture and/or oxygen can lead to oxidation of the feedstock powders and a reduction in the weld strength between layers, leading to premature failure of the components. Oxygen is therefore evacuated from the chamber and displaced with Argon before the laser bonding of the powdered layers begins. For similar product quality reasons, it is also critical that oxygen and moisture are measured in the production of the fine metal powders used as base material.

In both applications there is a significant safety aspect in measuring oxygen and moisture when handling large quantities of powdered metals. Oxygen must be maintained below explosive limits to avoid a dust explosion and so continuously measured. Even without the presence of oxygen and in standard inerting gases such as nitrogen or carbon dioxide, some metals can still ignite.

Moisture measurement is also critical as some metal powders (Al or Mg) will produce hydrogen and steam if mixed. In addition, damp metal powders are extremely dangerous and can produce a strong exothermic reaction leading to steam explosion if not properly identified.

Application

Oxygen and moisture are measured at two points along the 3D printing process, namely in the chamber of each 3D printing machine and at the production location of the fine metal power feedstock.

3D Printing Machine: Each 3D printing machine will have an oxygen measurement and most will be accompanied by a moisture measurement. These measurements are vital in detecting changes in the environment due to leakages, incomplete purges or contamination in base materials, the results of which can lead to a change in the mechanical and chemical properties of the components. These measurements are continuous throughout the 3D printing process where the atmosphere should remain stable except for changeover over events which will require a purging of the chamber.

Metal Powder Manufacturing:在金属粉末生产基地,进行类似的测量以避免污染原料产品。制造和储存通常可以在惰性气氛中发生,并且氩气是优选的气体给出它与氧气的惰性性质和高密度比。当某些金属仍然可以点燃时,诸如二氧化碳或氮的标准惰性气体可能是无效的。

Benefits:

  • Low maintenance and calibration requirements
  • Compact designs with integrated display
  • Fast response times and no background interference
  • Proven field performance in similar applications
  • Proven fuel cell technology
客户's Challenge

The challenge in OEM manufactured 3D printing machines lies in the size and reliability of the transmitters and their measurements. Space in 3D printing machines is a premium and so the measurement solution must have appropriate form factors and be free of interference from background gases such as nitrogen or argon. Printing times can be hours or days and so the transmitters must operate without the requirement for intervention while having a fast response time to allow the operator time to respond to changes in the internal chamber.

Panametrics' Solution

Oxy.iq非常适合使用VeriDri OEM溶液测量水分的同时氧气测量。两种发射机都采用Intry.iq的集成显示和控制适当大小,提供操作员易于校准和维护。此外,两个发射器的响应时间在识别通过氧气或湿气或湿气的抗噪声和典型的背景气体对测量的可靠性没有影响。

Application specifications

Moisture

  • Range: 0 - 1000 ppmV
  • Nominal: 50 ppmV

Oxygen

  • Range: 0 - 1000 ppmV
  • Nominal: 50 ppmV

Download the application note here

Learn more about Panametrics oxygen analyzers solution

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